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Reference type: Journal
Authors: Zhao T, Guan XJ, Tang WJ, Ma Y, Zhang HX
Article Title: Preparation of temperature sensitive molecularly imprinted polymer for solid-phase microextraction coatings on stainless steel fiber to measure ofloxacin.
Publication date: 2015
Journal: Analytica Chimica Acta
Volume: 853
Page numbers: 668-675.
DOI: 10.1016/j.aca.2014.10.019
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0003267014012525

Abstract: A kind of new temperature sensitive molecularly imprinted polymer (MIP) with ofloxacin (OFL) as template was prepared for the coating of solid phase microextraction (SPME). Dopamine was self-polymerized on stainless steel fiber (SSF) as the SPME support followed by silanization. Then MIP was synthesized as SPME coating on the modified SSF in a capillary, with N-isopropyl acrylamide as temperature sensitive monomer and methacrylic acid as functional monomer. The synthesis could be well repeated with multiple capillaries putting in the same reaction solution. The obtained MIP fiber was evaluated in detail with different techniques and various adsorption experiments. At last the MIP fiber was used to extract the OFL in milk. Satisfied recoveries between 89.7 and 103.4% were obtained with the limit of quantification (LOQLC) of 0.04 μg mL-1 by the method of SPME coupled with high performance of liquid chromatography (HPLC)
Template and target information: ofloxacin, OFL
Author keywords: molecularly imprinted polymer, solid phase microextraction, Ofloxacin, temperature sensitive


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