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Reference type: Journal
Authors: Rodríguez-Fernández R, Peña-Vázquez E, Bermejo-Barrera P
Article Title: Synthesis of an imprinted polymer for the determination of methylmercury in marine products.
Publication date: 2015
Journal: Talanta
Volume: 144
Page numbers: 636-641.
DOI: 10.1016/j.talanta.2015.06.028
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0039914015300758

Abstract: A molecularly imprinted polymer was synthesized using the precipitation method with methylmercury chloride as the template, phenobarbital as ligand, methacrylic acid (MMA) as monomer, and ethylene glycoldimethacrylate (EDMA) as cross-linking agent. The MIP was characterized using elemental analysis, infrared spectroscopy, energy dispersive X-ray fluorescence and scanning electron microscopy. The operating conditions for solid phase extraction (SPE) were optimized in column mode (pH, loading and elution flow rate using 1 M thiourea in 1 M HCl). The polymer was used for analyzing the toluene extracts of two reference materials (BCR-463 and TORT-2) with good accuracy
Template and target information: methylmercury
Author keywords: Methylmercury, molecularly imprinted polymer (MIP), SPE, HRCSAAS, Fish


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