MIPdatabase
Authors: Schwarz LJ, Danylec B, Harris SJ, Boysen RI, Hearn MTW
Article Title: Sequential molecularly imprinted solid-phase extraction methods for the analysis of resveratrol and other polyphenols.
Publication date: 2016
Journal: Journal of Chromatography A
Volume: 1438
Page numbers: 22-30.
DOI: 10.1016/j.chroma.2016.02.028
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0021967316301273
Abstract: Molecularly imprinted polymers (MIPs) templated with either the phytoalexin, (E)-resveratrol, or its structural analog, 3,5-dihydroxy-N-(4-hydroxyphenyl)benzamide, have been used in tandem for the sequential extraction of (E)-resveratrol from aqueous peanut meal extracts in high purity and in near quantitative yields. Re-processing of the (E)-resveratrol-depleted peanut meal extract with the 3,5-dihydroxy-N-(4-hydroxyphenyl)benzamide imprinted MIP yielded additional polyphenolic components, identified as A-type procyanidins. Tandem liquid chromatography-electrospray ionization mass spectrometry confirmed the identity and purity of the isolated products. This study documents the advantages of tandem approaches with MIPs for the solid phase extraction and analysis of multiple bioactive compounds present in complex biomass waste streams
Template and target information: (E)-resveratrol, 3,5-dihydroxy-N-(4-hydroxyphenyl)benzamide, A-type procyanidins, procyanidins
Author keywords: Molecularly imprinted polymers, molecularly imprinted solid-phase extraction, Polyphenolics, resveratrol, Procyanidins, Peanut meal
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