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Reference type: Journal
Authors: Ma JY, Chen B, Yao SZ, Liu C
Article Title: Synthesis of diethylstilbestrol-based molecularly imprinted polymers and its application in residues analysis.
Publication date: 2005
Journal: Chinese Journal of Analytical Chemistry
Volume: 33
Issue: (10)
Page numbers: 1413-1416.
Alternative URL: http://en.cnki.com.cn/Article_en/CJFDTotal-FXHX200510013.htm

Abstract: Using diethylstilbestrol (DES) as template molecule, α-methacrylic acid (MAA) as functional monomer, and ethylene dimethacrylate (EDMA) as crosslinking agent, a polymer was synthesized by molecular imprinting technique. The molecularly imprinted polymers (MIPs) were loaded into the solid-phase(extraction) (SPE) cartridge,which was applied to the pretreatment of residues analysis of diethylstilbestrol.(Elution) conditions of DES on the solid-phase extraction cartridge were optimized.Furthermore,the difference of the retention characteristics of diethylstilbestrol on the C_(18) and DES-MIPs solid-phase extraction cartridge was compared.The DES-MIPs-SPE had higher selectivity than the C_(18)-SPE.The method has been applied to pretreat spiked samples successfully with the recovery more than 95%.
Template and target information: diethylstilbestrol, DES
Author keywords: molecularly imprinted polymer, Solid-phase extraction, diethylstilbestrol


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