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Reference type: Journal
Authors: Koohpaei AR, Shahtaheri SJ, Ganjali MR, Forushani AR, Golbabaei F
Article Title: Optimization of solid-phase extraction using developed modern sorbent for trace determination of ametryn in environmental matrices.
Publication date: 2009
Journal: Journal of Hazardous Materials
Volume: 170
Issue: (2-3)
Page numbers: 1247-1255.
DOI: 10.1016/j.jhazmat.2009.05.125
Alternative URL: http://www.sciencedirect.com/science/article/B6TGF-4WGK4N4-G/2/27eaa66fa8e90ad2a859c9d4e31640b3

Abstract: In recent years, there has been a significant increase in molecularly imprinted solid-phase extraction (MISPE) technique for the purification and clean-up of environmental samples. In this study, solid-phase extraction using the imprinted polymer has been optimized with the experimental design approach for a triazine herbicide, named ametryn with regard to the critical factors such as sample pH, sample concentration, sample flow-rate, sample volume, elution solvent, washing solvent and sorbent mass. These factors were evaluated statistically and also validated with spiked drinking water samples and showed a good reproducibility over six consecutive days as well as six within-day experiments. Also, in order to the evaluate efficiency of the optimized MISPE protocols, enrichment capacity, reusability and cross-reactivity of cartridges have been studied. Finally, a selective MISPE was successfully demonstrated for ametryn with a recovery of above 90% for spiked drinking water samples. It was concluded that the central composite design could prove beneficial for aiding the MIP and MISPE development
Template and target information: ametryn
Author keywords: MISPE, Central composite design, water samples, herbicides, Ametryn


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