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Reference type: Journal
Authors: Franqui LS, Vieira AC, Maia PP, Figueiredo EC
Article Title: Molecularly imprinted solid-phase extraction of urinary trans-trans muconic acid and analysis by gas chromatography-mass spectrometry.
Publication date: 2012
Journal: Quimica Nova
Volume: 35
Issue: (8)
Page numbers: 1577-1581.
DOI: 10.1590/S0100-40422012000800016

Abstract: This paper describes selective molecularly imprinted solid-phase extraction of ttMA from urine samples followed by derivatization and analysis by gas chromatography/mass spectrometry (GC/MS). The analytical calibration curve ranged from 0.3 to 7.0 mg L-1 (r = 0.999) and the limit of quantitation (LOQ) was 0.3 mg L-1. The method was applied for the determination of ttMA in urine samples from smokers and concentrations detected ranged from < LOQ to 1.64 mg L-1. Thus, the proposed method proved adequate for the determination of urinary ttMA in the biomonitoring of occupational exposure to low levels of benzene
Template and target information: trans-trans muconic acid, ttMA
Author keywords: gas chromatography, mass spectrometry, Molecularly imprinted polymers, Trans-trans-muconic acid

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