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Reference type: Journal
Authors: Zhang HY, Wei YW, Zhou JH, Xu ZX, Tian S, Huang H, He JX
Article Title: Preparation and Application of a Molecular Imprinting Matrix Solid Phase Dispersion Extraction for the Determination of Olaquindox in Chicken by High Performance Liquid Chromatography.
Publication date: 2013
Journal: Food Analytical Methods
Volume: 6
Issue: (3)
Page numbers: 915-921.
DOI: 10.1007/s12161-012-9502-7

Abstract: In this paper, a new method was established to extract olaquindox in chicken by matrix solid phase dispersion extraction using the molecularly imprinted polymers as solid phase materials. The polymers were prepared using olaquindox as the template, methacrylic acid as the functional monomer, and ethylene glycol dimethacrylate as the cross-linking agent. The imprinted material was characterized by static and kinetic adsorption experiments. The results showed that it had good recognition, selective ability, and fast adsorption-desorption dynamics for olaquindox. The prepared material was used as solid phase materials of matrix solid phase dispersion to enrich the olaquindox and then determined by high performance liquid chromatography. Under the optimized conditions, the range of recovery spiked with olaquindox at 1.0 and 2.0 μg g-1 levels was between 85.3 and 93.2 %
Template and target information: olaquindox
Author keywords: molecular imprinting technique, Olaquindox, Matrix solid phase dispersion


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