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Reference type: Journal
Authors: Shakerian F, Dadfarnia S, Shabani AMH
Article Title: Synthesis of nano-pore size Al(III)-imprinted polymer for the extraction and preconcentration of aluminum ions.
Publication date: 2013
Journal: Journal of the Iranian Chemical Society
Volume: 10
Issue: (4)
Page numbers: 669-676.
DOI: 10.1007/s13738-012-0199-8

Abstract: In this study, an ion imprinted polymer (IIP) was prepared for the selective separation and preconcentration of trace levels of aluminum. Al(III) IIP was synthesized in the presence of Al(III)-8-hydroxyquinoline (oxine) complex using styrene and ethylene glycol dimethacrylate as a monomer and crosslinker, respectively. The imprinted Al(III) ions were completely removed by leaching the IIP with HCl (50 % v/v) and were characterized by FTIR and scanning electron microscopy. The maximum sorption capacity for Al(III) ions was found to be 3.1 mg g-1 at pH 6.0. Variables affecting the IIP solid phase extraction were optimized by the univariable method. Under the optimized conditions, a sample volume of 400 mL resulted in an enhancement factor of 194. The detection limit (defined as 3 S b/m) was found to be 1.6 μg L-1. The method was successfully applied to the determination of aluminum in natural water, fruit juice and cow milk samples
Template and target information: aluminium ion, AL(III)
Author keywords: ion imprinted polymer, Aluminum, solid phase extraction, Fruit juices, Cow milk

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