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Reference type: Journal
Authors: Naeimi H, Nejadshafiee V, Islami MR
Article Title: Designable Metal/PMO Nanocomposite and Preparation by a Surface Imprinting Technique Combined with a Sol-Gel Process for Catalytic Click Reaction.
Publication date: 2016
Journal: Bulletin of the Chemical Society of Japan
Volume: 89
Issue: (2)
Page numbers: 212-219.
DOI: 10.1246/bcsj.20150291
Alternative URL: https://www.jstage.jst.go.jp/article/bcsj/89/2/89_20150291/_article

Abstract: Novel metal/periodic mesoporous organosilica nanocomposites were prepared through metal template (Cu, Zn, Ni, and Co) imprinted ligand into periodic mesoporous organosilica (PMO) and their application as a recyclable catalyst in click synthesis of β-hydroxytriazoles described. The structure of the nanocomposite was characterized by X-ray diffraction (XRD), Fourier transform-infrared (FT-IR) spectroscopy, N2 adsorption-desorption analysis, scanning electron microscopy (FE-SEM), energy-dispersive spectrometer (EDS), and thermogravimetric analysis (TGA). The results showed that the copper-imprinted periodic mesoporous organosilica nanocomposite (Cu/PMO NC) as a catalyst had good catalytic activity and short reaction times toward the multicomponent reaction for synthesis of β-hydroxytriazoles. Furthermore, the catalyst was regenerated and reused in the reaction for six cycles
Template and target information: copper, zinc, nickel, cobalt, Cu, Zn, Ni, Co

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