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Reference type: Journal
Authors: Ji WH, Chen LX, Ma XL, Wang X, Gao QS, Geng YL, Huang LQ
Article Title: Molecularly imprinted polymers with novel functional monomer for selective solid-phase extraction of gastrodin from the aqueous extract of Gastrodia elata.
Publication date: 2014
Journal: Journal of Chromatography A
Volume: 1342
Page numbers: 1-7.
DOI: 10.1016/j.chroma.2014.03.046
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0021967314004579

Abstract: Molecular imprinted polymers (MIPs) with high selectivity and affinity to gastrodin in water were designed using allyl 2,3,4,6-tetra-O-acetyl-glucopyranoside (TAGL) and 1,2,3,4,5-pentafluoro-6-vinylbenzene (PFVB) as novel functional monomers. Binding characterization of pre-polymerization complexes was researched by nuclear magnetic resonance (NMR) and the MIPs were characterized by scanning electron microscopy (SEM). The properties involving adsorption isotherm, adsorption kinetics and selective recognition capacity were evaluated. The MIPs/TAGL exhibited good site accessibility in which it only took 30 min to achieve adsorption equilibrium and highly selective recognition for the template. Furthermore, the performance of the MIPs/TAGL as solid phase extraction material was investigated in detail and hot water at 50 C served as the eluting solvent. Pure gastrodin with the recovery of 76.6% was obtained from the aqueous extract of Gastrodia elata roots
Template and target information: gastrodin
Author keywords: molecular imprinted polymers, Gastrodin, Solid-phase extraction, Novel functional monomer


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