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Reference type: Journal
Authors: Zhang C, Cai JR, Duan YQ, Xu L, Fang GZ, Wang S
Article Title: Synthesis, characterization and application of organic-inorganic hybrid and carbaryl-imprinted capillary monolithic column.
Publication date: 2014
Journal: Chemical Research in Chinese Universities
Volume: 30
Issue: (3)
Page numbers: 374-378.
DOI: 10.1007/s40242-014-3420-8

Abstract: Organic-inorganic hybrid and carbaryl-imprinted capillary monolith was synthesized via methacrylic acid(MAA) as functional monomer, γ-methacryloxypropyltrimethoxysilane(γ-MAPS) as crosslinker and carbaryl as template molecule in an acetonitrile/dichloromethane mixture(1:4, volume ratio). With the capillary column obtained from this monolith, three carbamates(carbaryl, fenobucarb and metolcarb) were separated effectively by electrochromatography with the kMIP/kNIP values of 7.57, 1.27 and 1.64, respectively. In 20 mmol/L phosphate buffer solution (pH=3.5) with 30% (volume fraction) of acetonitrile, carbaryl was separated directly from the three-carbamate mixture (carbaryl, fenobucarb and metolcarb) with an effective 15 cm-length imprinted column
Template and target information: carbaryl
Author keywords: organic-inorganic hybrid, Carbaryl-imprinted capillary, monolith, Separate

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