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Reference type: Journal
Authors: Liu XY, Yu D, Yu YC, Ji SJ
Article Title: Preparation of a magnetic molecularly imprinted polymer for selective recognition of rhodamine B.
Publication date: 2014
Journal: Applied Surface Science
Volume: 320
Page numbers: 138-145.
DOI: 10.1016/j.apsusc.2014.08.122
Alternative URL: http://www.sciencedirect.com/science/article/pii/S016943321401900X

Abstract: A novel magnetic molecularly imprinted polymer (MMIP) was developed as an adsorbent to selectively remove rhodamine B from real samples. The polymer was characterized by scanning electron microscopy, Fourier-transform infrared spectroscopy, and thermo-gravimetric analysis. Static adsorption, kinetic adsorption, and selective recognition experiments were also performed to investigate the specific adsorption equilibrium, kinetics, and selective recognition ability of the MMIP. The MMIPs had outstanding thermal stability, large adsorption capacity, and high competitive selectivity. When they were used as dispersed solid-phase extraction adsorbents in real samples, rhodamine B recovery was 79.97-81.88% and 75.56-79.74% in intra-day and inter-day reproducibility experiments with relative standard deviations lower than 2.62% and 4.28%, respectively. Extraction was optimized for yield and efficiency. Precision, accuracy, and linear working range were determined under optimal experimental conditions. The limits of detection and quantification were 1.05 and 3.49 μg L-1, respectively. These results suggest MMIPs may be used for determination of rhodamine B in real samples
Template and target information: rhodamine B
Author keywords: Rhodamine B, Magnetic molecularly imprinted polymer, Fluorospectrophotometry


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