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Reference type: Journal
Authors: Naraghi K, Panahi HA, Hassani AH, Moniri E
Article Title: Ion imprinted activated carbon solid-phase extraction coupled to flame atomic absorption spectrometry for selective determination of lead ions in environmental samples.
Publication date: 2014
Journal: Korean Journal of Chemical Engineering
Volume: 31
Issue: (10)
Page numbers: 1818-1823.
DOI: 10.1007/s11814-014-0104-5

Abstract: A simple lead ion imprinted sorbent was synthesized by coupling activated carbon with a known metal chelating compound, iminodiacetic acid. The ion imprinted sorbent has been characterized using Fourier transform infrared spectroscopy, elemental analysis and thermogravimetric analysis and subjected for the extraction and determination of trace Pb(II) in environmental water samples. The optimum pH value for sorption of the lead ion was 6.5. The sorption capacity of lead imprinted sorbent was 42.2 mg g-1. The chelating imprinted sorbent can be reused for five cycles of sorption-desorption without any significant change in sorption capacity. Compared with non-imprinted polymer particles, the lead ion imprinted sorbent showed high adsorption capacity, significant selectivity, good site accessibility for Pb(II). The equilibrium adsorption data of Pb(II) by modified resin were analyzed by Langmuir, Freundlich, Temkin and Redlich-Peterson models
Template and target information: lead ion, Pb(II)
Author keywords: solid phase extraction, polymer grafting, Lead (II), preconcentration, Isotherm study


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