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Reference type: Journal
Authors: Zhang LM, Wei XP, Wei YX, Li JP, Zeng Y
Article Title: Determination of Trace Gibberellin A3 by Magnetic Self-assembly Molecularly Imprinted Electrochemical Sensor.
Publication date: 2014
Journal: Chinese Journal of Analytical Chemistry
Volume: 42
Issue: (11)
Page numbers: 1580-1585.
DOI: 10.1016/S1872-2040(14)60780-5
Alternative URL: http://210.14.121.5:8080/fxhx/EN/abstract/abstract13701.htm

Abstract: Magnetic Fe3O4 nanoparticles were synthesized by co-precipitation method, and then magnetic Fe3O4@Au nanoparticle were synthesized to improve the affinity of particle surface. L-Cys-GA3 was grafted on the particle surface by self-assembly method, and then dropped it on glass carbon electrode. The MIP/Fe3O4@Au was further fabricated by electropolymerization of L-Cys. The surface morphology and particle size distribution of the Fe3O4@Au particle were studied by TEM. The structure and composition of GA3, MIP and nMIP were studied by IR. Under the optimum conditions including 30 cycles of electropolymerization period, 5 min of elution time, 7 min of rebinding time and with acetic acid-methanol (1:8, V/V) mixed solution as eluent, high stability and good recognition ability for GA3 were obtained through the sensor. The results showed that the concentration of GA3 in the range of 1.0 x 10-11 - 1.0 x 10-8 M had a linear relationship with the intensity of the oxidation peak current, with the detection limit of 2.6 x 10-12 M. The sensor was successfully used for the determination of GA3 in beer sample
Template and target information: gibberellin A3, GA3
Author keywords: Molecular imprinted, Gibberellins acid 3, self-assembly, magnetic nanoparticle


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