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Reference type: Journal
Authors: Chrzanowska AM, Poliwoda A, Wieczorek PP
Article Title: Characterization of particle morphology of biochanin A molecularly imprinted polymers and their properties as a potential sorbent for solid-phase extraction.
Publication date: 2015
Journal: Materials Science and Engineering: C
Volume: 49
Page numbers: 793-798.
DOI: 10.1016/j.msec.2015.01.069
Alternative URL: http://www.sciencedirect.com/science/article/pii/S092849311500079X

Abstract: Molecularly imprinted polymers (MIPs) with biochanin A as a template were obtained using a bulk polymerization with non-covalent imprinting approach. The polymers were prepared in acetonitrile as porogen, using ethylene glycol dimethacrylate (EDMA) as cross-linking agent. The synthesis, with an application of 1',1'-azobis(cyclohexanecarbonitrile) (ACHN) as an initiator, has been performed thermally. During the synthesis process the effect of different functional monomers such as methacrylic acid (MAA), acrylamide (AA) and 4-vinylpyridine (4-VP) was investigated. The application of nitrogen sorption porosimetry, scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) permitted the characterization and evaluation of synthesized polymers. The adsorption capacity of obtained MIPs was checked by using the binding testing. All synthesized polymers were evaluated as solid-phase extraction (SPE) sorbents for isolation and preconcentration of biochanin A and its analogues, daidzein and genistein. The MIPs exhibited higher affinity for biochanin A over competitive compounds
Template and target information: biochanin A
Author keywords: Phytoestrogens, molecular imprinting, adsorption, Solid-phase extraction


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