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Reference type: Journal
Authors: Feng QZ, Zhao LX, Yan W, Lin JM, Zheng ZX
Article Title: Molecularly imprinted solid-phase extraction combined with high performance liquid chromatography for analysis of phenolic compounds from environmental water samples.
Publication date: 2009
Journal: Journal of Hazardous Materials
Volume: 167
Issue: (1-3)
Page numbers: 282-288.
DOI: 10.1016/j.jhazmat.2008.12.115
Alternative URL: http://www.sciencedirect.com/science/article/B6TGF-4V8GB8F-D/2/eab075223ba4fc38b80da0d0a9745f04

Abstract: The molecularly imprinted bulk polymer with 2,4,6-trichlorophenol (2,4,6-TCP) as the template molecule and methylacrylic acid (MAA), ethylene glycol dimethacrylate (EGDMA) as functional monomer and the crosslinker, respectively, has been prepared and applied to the molecularly imprinted solid-phase extraction (MISPE) procedure for selective preconcentration of phenolic compounds from environmental water samples. Various parameters affecting the extraction efficiency of the polymer have been evaluated to optimize the selective preconcentration of the phenolic compounds from aqueous samples. The characteristics of the MISPE method were valided by HPLC. The recoveries ranged between 90% and 98% (RSD: 0.9-2.3%, n=3) for tap water, between 85% and 105% (RSD: 2.6-4.9%, n=3) for river water, between 78% and 98% (RSD: 2.6-5.4%, n=3) for sewage water fortified with 0.4mgL-1 of phenol, 4-chlorophenol (4-CP), 2,4-dichlorophenol (2,4-DCP), pentachlorophenol (PCP). It was demonstrated that this MISPE-HPLC method could be applied to direct preconcentration and determination of phenolic compounds in environmental water samples
Template and target information: 2,4,6-trichlorophenol, 2,4,6-TCP
Author keywords: molecularly imprinted polymer, 2,4,6-Trichlorophenol, phenolic compounds, molecularly imprinted solid-phase extraction, high performance liquid chromatography

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