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Reference type: Journal
Authors: Zhang ZH, Zhang HB, Luo LJ, Hu YF, Nie LH
Article Title: Preparation and Application of Multi-walled Carbon Nanotube Surface Benzoyl Peroxide Imprinted Composite Solid-phase Extraction Materials.
Publication date: 2009
Journal: Acta Chimica Sinica
Volume: 67
Issue: (24)
Page numbers: 2833-2839.
Alternative URL: http://sioc-journal.cn/Jwk_hxxb/EN/abstract/abstract338465.shtml

Abstract: A novel composite imprinted material based on multi-wall carbon nanotubes (MWNT) was synthesized successfully with a surface polymerization method using benzoyl peroxide (BPO) as a template molecule, methacrylic acid (MAA) as functional monomers, ethylene glycol dimethacrylate (EGDMA) as cross-linkers. The molecularly imprinted polymers (MIP) based on the surface of MWNT was characterized by infrared spectroscopy (IR), differential thermal analysis (DTA) and scanning electron microscopy (SEM), and the results suggested that MIP was grafted to the surface of MWNT successfully. The adsorption amount of benzoyl peroxide by MIP was measured by high performance liquid chromatography (HPLC) and equilibrium binding experiment. A kind of binding site was observed for MIP to BPO with the maximum apparent binding constant of 56.20 mu mol/g. Being used as solid-phase extraction materials, the imprinted polymers extracted benzoyl peroxide from flour successfully with the concentration enrichment factor of 526
Template and target information: benzoyl peroxide
Author keywords: molecularly imprinted polymer, multi-walled carbon nanotube, benzoyl peroxide, high performance liquid chromatography


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