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Reference type: Journal
Authors: Yang X, Wang RL, Wang WH, Yan HY, Qiu MD, Song YX
Article Title: Synthesis of a novel molecularly imprinted organic-inorganic hybrid polymer for the selective isolation and determination of fluoroquinolones in tilapia.
Publication date: 2014
Journal: Journal of Chromatography B
Volume: 945-946
Page numbers: 127-134.
DOI: 10.1016/j.jchromb.2013.11.040
Alternative URL: http://www.sciencedirect.com/science/article/pii/S1570023213006533

Abstract: A novel molecularly imprinted organic-inorganic hybrid polymer (MI-MAA/APTS) based on a dummy molecular imprinting technique and an organic-inorganic hybrid material technique was synthesised and used as a sorbent in solid-phase extraction for the selective isolation and determination of ofloxacin (OFL), lomefloxacin (LOM), and ciprofloxacin (CIP) in tilapia samples. The MI-MAA/APTS sorbent was prepared from 3-aminopropyltriethoxysilanes (APTS) as an inorganic source and methacrylic acid (MAA) as an organic source and exhibited high mechanical strength and special affinities to the analytes. A comparison of MI-MAA/APTS with other conventional sorbents (C18 and HLB) showed that MI-MAA/APTS displayed good selectivity and affinity for OFL, LOM, and CIP, and the recoveries of the analytes at three spiked levels were in the range of 85.1-101.0%, with the relative standard deviations G5.1%. The presented MI-MAA/APTS-SPE-HPLC method could be potentially applied to the determination of fluoroquinolones (FQs) in complex fish samples
Template and target information: ofloxacin, OFL, lomefloxacin, LOM, ciprofloxacin, CIP, fluoroquinolones, FQs
Author keywords: Organic-inorganic hybrid materials, molecular imprinting, Solid-phase extraction, Fluoroquinolones, Tilapia

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