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Authors: Lian ZR, Liang ZL, Wang JT
Article Title: Selective extraction and concentration of mebendazole in seawater samples using molecularly imprinted polymer as sorbent.
Publication date: 2015
Journal: Marine Pollution Bulletin
Volume: 91
Issue: (1)
Page numbers: 96-101.
DOI: 10.1016/j.marpolbul.2014.12.022
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0025326X14008236
Abstract: A high selective pre-treatment method for the extraction and analysis of mebendazole in environmental water samples was developed based on molecularly imprinted solid-phase extraction (MISPE). The mebendazole imprinted polymers were synthesized in acetonitrile using methacrylic acid and ethylene glycol dimethacrylate as functional monomer and cross-linker respectively. The imprinted materials showed high adsorption ability for mebendazole and were applied as special solid-phase extraction sorbents for selective separation of mebendazole. An off-line MISPE procedure was developed for the purification and enrichment of mebendazole from natural seawater samples prior to high-performance liquid chromatography analysis. The recoveries of spiked seawater on the MISPE cartridges were from 83.0% to 90.6%, and the values of the relative standard deviation were in the range of 2.78-4.13% (n = 3). The satisfied results showed that this pre-treatment methodology for extracting mebendazole in seawater was simple and effective
Template and target information: mebendazole
Author keywords: Mebendazole, molecularly imprinted polymer, adsorption, Solid-phase extraction, natural seawater
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