MIPs logo MIPdatabase      MIP2024 Conference banner, website is now open, register on site for important updates   
Custom Search
Reference type: Journal
Authors: Moreno-González D, Lara FJ, Jurgovská N, Gámiz-Gracia L, García-Campaña AM
Article Title: Determination of aminoglycosides in honey by capillary electrophoresis tandem mass spectrometry and extraction with molecularly imprinted polymers.
Publication date: 2015
Journal: Analytica Chimica Acta
Volume: 891
Page numbers: 321-328.
DOI: 10.1016/j.aca.2015.08.003
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0003267015009812

Abstract: A new analytical method based on capillary zone electrophoresis-tandem mass spectrometry is proposed and validated for the identification and simultaneous quantification of nine aminoglycosides in honey samples. Detection using an ion trap mass analyzer operating in the multiple reaction monitoring mode was used. Different parameters were optimized in order to obtain an adequate separation combined with the highest sensitivity. In order to achieve high selectivity in the sample treatment, a commercially-available molecularly imprinted polymer has been used for the solid phase extraction of the analytes. Under optimum conditions, recoveries for fortified samples ranged from 88.2 to 99.8%, with relative standard deviations lower than 8%. The limits of detection ranged from 0.4 to 28.5 μg kg-1. Furthermore, the decision limit and the detection capability were evaluated, ranging from 3.5 to 60.5 μg kg-1 and from 6.0 to 103.1 μg kg-1, respectively, demonstrating the sensitivity and applicability of this fast and simple method
Template and target information: aminoglycosides, commercial MIP
Author keywords: Aminoglycosides, capillary zone electrophoresis, tandem mass spectrometry, stacking, Molecularly imprinted polymers, Honey


  Template of Doom spoof movie poster bag  Chemistry peptide mug  Chemists are fun customisable shirt






 

Join the Society for Molecular Imprinting
Logo of the Society for Molecular Imprinting

New items RSS feed
new items RSS feed  View latest updates

Sign-up for e-mail updates:
Choose between receiving an occasional newsletter or more frequent e-mail alerts.
Click here to go to the sign-up page.


Is your name elemental or peptidic? Enter your name and find out by clicking either of the buttons below!
Other products you may like:
view listings for MIP books on eBay:



Mickey Mouse 90th Anniversary banner