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Reference type: Journal
Authors: Díaz-Álvarez M, Smith SP, Spivak DA, Martín-Esteban A
Article Title: Preparation of molecularly imprinted polymeric fibers using a single bifunctional monomer for the solid-phase microextraction of parabens from environmental solid samples.
Publication date: 2016
Journal: Journal of Separation Science
Volume: 39
Issue: (3)
Page numbers: 552-558.
DOI: 10.1002/jssc.201500967

Abstract: In this study, molecularly imprinted polymer fibers for solid-phase microextraction have been prepared with a single bifunctional monomer, N,O-bismethacryloyl ethanolamine using the so-called "one monomer molecularly imprinted polymers" method, replacing the conventional combination of functional monomer and cross-linker to form high fidelity binding sites. For comparison, imprinted fibers were prepared following the conventional approach based on ethylene glycol dimethacrylate as cross-linker and methacrylic acid as monomer. The recognition performance of the new fibers was evaluated in the solid-phase microextraction of parabens, and from this study it was concluded that they provided superior performance over conventionally formulated fibers. Ultimately, real-world environmental testing on spiked solid samples was successful by the molecularly imprinted solid-phase microextraction of samples, and the relative recoveries obtained at enrichment levels of 10 ng/g of parabens were within 78-109% for soil and 83-109% for sediments with a relative standard deviation <15% (n = 3)
Template and target information: parabens
Author keywords: Environmental solid samples, Molecularly imprinted fibers, Parabens, solid-phase microextraction

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