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Reference type: Journal
Authors: Yan L, Yin YL, Lv PP, Zhang ZH, Wang J, Long F
Article Title: Synthesis and Application of Novel 3D Magnetic Chlorogenic Acid Imprinted Polymers Based on a Graphene-Carbon Nanotube Composite.
Publication date: 2016
Journal: Journal of Agricultural and Food Chemistry
Volume: 64
Issue: (15)
Page numbers: 3091-3100.
DOI: 10.1021/acs.jafc.6b00518

Abstract: A novel three-dimensional (3D) magnetic chlorogenic acid (CGA) imprinted polymer (MMIP) was prepared with novel carbon hybrid nanocomposite as the carrier, chlorogenic acid as the template molecule, and methacrylic acid as the functional monomer. The 3D MMIPs were characterized by scanning electron microscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis, vibrating sample magnetometer, and UV spectrometry in detail. The results showed that the imprinted layer was attached successfully on the surface of a 3D magnetic carbon hybrid nanocomposite. The adsorption performance of the 3D MMIPs was investigated, and the results showed that the 3D MMIPs exhibited high adsorption capacity and fast adsorption rate toward CGA with a maximum adsorption capacity of 10.88 mg g-1. The extraction conditions involving washing solvent, the pH of eluent solvent, elution volume, and desorption time were also investigated in detail. Combined with high-performance liquid chromatography, the 3D MMIPs have been applied to successfully extract CGA from Eucommia leaf extract samples
Template and target information: chlorogenic acid, CGA
Author keywords: 3D molecularly imprinted polymers, Graphene, carbon nanotubes, chlorogenic acid, Magnetic solid-phase extraction

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