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Reference type: Journal
Authors: Van Royen G, Dubruel P, Van Weyenberg S, Daeseleire E
Article Title: Evaluation and validation of the use of a molecularly imprinted polymer coupled to LC-MS for benzylpenicillin determination in meat samples.
Publication date: 2016
Journal: Journal of Chromatography B
Volume: 1025
Page numbers: 48-56.
DOI: 10.1016/j.jchromb.2016.05.003
Alternative URL: http://www.sciencedirect.com/science/article/pii/S1570023216303075

Abstract: This article describes a full analytical method for the clean-up and detection of benzylpenicillin in chicken and beef meat samples using a previously developed molecularly imprinted polymer in a solid-phase extraction cleanup step followed by analysis using LC-MS/MS. The method was validated based on the criteria and the requirements of the European Commission Decision 2002/657/EC. This validation revealed method performance characteristics that meet all the criteria in the Decision with limits of detection for chicken and beef meat samples of 6.2 and 14.4 μg/kg, respectively, 8 and 3.5 times lower than the MRL. This method holds strong potential when a specific cleanup of benzylpenicillin is required, because with slight modifications it is also applicable in a milk matrix [1]
Template and target information: benzylpenicillin
Author keywords: molecularly imprinted polymer, Benzylpenicillin, MISPE, Meat, Validation


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