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Reference type: Journal
Authors: Areerob Y, Sricharoen P, Limchoowong N, Chanthai S
Article Title: Core-shell SiO2-coated Fe3O4 with a surface molecularly imprinted polymer coating of folic acid and its applicable magnetic solid-phase extraction prior to determination of folates in tomatoes.
Publication date: 2016
Journal: Journal of Separation Science
Volume: 39
Issue: (15)
Page numbers: 3037-3045.
DOI: 10.1002/jssc.201600342

Abstract: A novel core-shell magnetic surface molecularly imprinted polymer with folic acid as a template was successfully synthesized by the sol-gel method. To generate Lewis acid sites in the silica matrix for the interaction of the metal coordinate with the template, 3-aminopropyltriethoxysilane was used as a functional monomer, tetraethyl orthosilicate as a cross-linker, and aluminum ions as a dopant. The magnetite encapsulated by the silica shell plays an important role as a magnetic-coated polymer. The synthesized product was characterized by powder X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and FTIR and UV/Vis spectroscopy. The powder X-ray diffraction patterns, FTIR and UV/Vis spectra confirmed the characteristics of the as-prepared silica coated magnetite and folic acid molecularly imprinted polymer. It was successfully applied for magnetic solid-phase extraction prior to the determination of folates in tomato samples using high-performance liquid chromatography with photodiode array detection. The detection limit of the proposed method was 1.67 μg/L, and results were satisfactory, with a relative standard deviation of < 3.94%
Template and target information: folic acid
Author keywords: Folic acid, Magnetic solid-phase extraction, molecularly imprinted polymer, sol-gel method


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