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Reference type: Journal
Authors: Kiani A, Ghorbani M
Article Title: Synthesis of core-shell magnetic ion-imprinted polymer nanospheres for selective solid-phase extraction of Pb2+ from biological, food, and wastewater samples.
Publication date: 2017
Journal: Journal of Dispersion Science and Technology
Volume: 38
Issue: (7)
Page numbers: 1041-1048.
DOI: 10.1080/01932691.2016.1219666

Abstract: Magnetic ion-imprinted polymer nanospheres, which have core-shell structures, have been synthesized as an adsorbent for extraction of Pb2+ from real samples prior to its flame atomic absorption spectrometric determination. The prepared adsorbent has been characterized using XRD, VSM, TEM, and FTIR measurements. The optimization results revealed that the adsorbent exhibited high selectivity toward Pb2+ over other cations such as Cu2+ and Zn2+. In addition, the removal efficiency of synthesized adsorbent was considerable (qm = 171.42 mg g-1), its calibration curve was linear (0.5 - 850.0 ng mL-1), and detection limit was 0.01 ng mL-1. These results suggested that the prepared nanoadsorbent is an ideal candidate for solid-phase extraction of Pb2+ ions
Template and target information: lead ion, Pb(II)
Author keywords: flame atomic absorption spectrometry, Ion-imprinted polymer, lead ions, magnetite nanospheres, solid phase extraction


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