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Reference type: Journal
Authors: Han YH, Yang CL, Zhou Y, Han DD, Yan HY
Article Title: Ionic Liquid-Hybrid Molecularly Imprinted Material-Filter Solid-Phase Extraction Coupled with HPLC for Determination of 6-Benzyladenine and 4-Chlorophenoxyacetic Acid in Bean Sprouts.
Publication date: 2017
Journal: Journal of Agricultural and Food Chemistry
Volume: 65
Issue: (8)
Page numbers: 1750-1757.
DOI: 10.1021/acs.jafc.6b03922

Abstract: A new method involving ionic liquid-hybrid molecularly imprinted material-filter solid-phase extraction coupled to high-performance liquid chromatography (IL-HIM-FSPE-HPLC) was developed for the simultaneous isolation and determination of 6-benzyladenine (6-BA) and 4-chlorophenoxyacetic acid (4-CPA) in bean sprouts. Sample preconcentration was performed using a modified filter, with the new IL-HIM as the adsorbent, which shows double adsorption. The first adsorption involves special recognition of molecular imprinting, and the second involves ion exchange and electrostatic attraction caused by the ionic liquid. This method combines the advantages of ionic liquids, hybrid materials, and molecularly imprinted polymers and was successfully applied to determine 6-BA and 4-CPA in bean sprouts. The adsorption of 6-BA to IL-HIM is based on selective imprinted recognition, whereas the adsorption of 4-CPA is mainly dependent on ion-exchange interactions
Template and target information: 6-benzyladenine, 6-BA, 4-chlorophenoxyacetic acid, 4-CPA
Author keywords: 4-chlorophenoxyacetic acid, 6-benzyladenine, Bean sprouts, filter solid-phase extraction, ionic liquid-hybrid molecularly imprinted polymer

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