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Reference type: Journal
Authors: Huang HL, Zhang CB, Liu L, Wang ZH
Article Title: Synthesis and characterization of a novel quercetin magnetic molecularly imprinted polymer via reversible addition fragmentation chain transfer strategy.
Publication date: 2017
Journal: Journal of Macromolecular Science, Part A
Volume: 54
Issue: (7)
Page numbers: 446-451.
DOI: 10.1080/10601325.2017.1320748

Abstract: Molecularly imprinted polymer (MIP) will be modified on the surface of the core-shell structure silica magnetic nanoparticles, during which quercetin is used as a template molecule, acrylamide as a functional monomer, azo-bisisobutyronitrile as an initiator and ethylene glycol dimethacrylate as a cross-linker, to synthesize highly efficient and selective quercetin magnetic molecularly imprinted nanoparticles via Reversible Addition-Fragmentation chain Transfer (RAFT) polymerization. FT-IR and X-ray diffraction (XRD) patterns are used to monitor the reaction and show the characteristic groups of each reaction step. Compared with the conventional bulk polymerization (2.7029 mg/g), the adsorption test showed that the MMIP by RAFT activity controlled polymerization had better absorption capacity for quercetin which the saturated adsorption amount was 4.8471 mg/g. Kinetic studies indicate that pseudo first order model is suitable to describe the adsorption mechanism. Thermodynamics experiment revealed that Langmuir model was more applied for explains the adsorption of quercetin onto magnetic molecularly imprinted polymer
Template and target information: quercetin
Author keywords: kinetics, Magnetic molecularly imprinted polymer, quercetin, RAFT, thermodynamics


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