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Reference type: Journal
Authors: Xu WZ, Zhang XM, Huang WH, Luan Y, Yang YF, Zhu MY, Yang WM
Article Title: Synthesis of surface molecular imprinted polymers based on carboxyl-modified silica nanoparticles with the selective detection of dibutyl phthalate from tap water samples.
Publication date: 2017
Journal: Applied Surface Science
Volume: 426
Page numbers: 1075-1083.
DOI: 10.1016/j.apsusc.2017.07.241
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0169433217322419

Abstract: In this work, the molecular imprinted polymers were synthesized with the low monomer concentrations for dibutyl phthalate (DBP). The polymers were prepared over carboxyl-modified silica nanoparticle, which used methacrylic acid as the functional monomer, ethylene glycol dimethacrylate as the cross-linker agent and azoisobutyronitrile as the initiator in the process of preparation. Various measures were used to characterize the structure and morphology in order to get the optimal polymer. The characterization results show that the optimal polymer has suitable features for further adsorption process. And adsorption capacity experiments were evaluated to analyze its adsorption performance, through adsorption isotherms/kinetics, selectivity adsorption and desorption and regeneration experiments. These results showed that the molecular imprinted polymers had a short equilibrium time about 60 min and high stability with 88% after six cycles. Furthermore, the molecular imprinted polymers were successfully applied to remove dibutyl phthalate. The concentration range was 5.0-30.0 μmol L-1, and the limit of detection was 0.06 μmol L-1 in tap water samples
Template and target information: dibutyl phthalate, DBP
Author keywords: molecular imprinted polymers, Dibutyl phthalate, selective adsorption, nanoparticles

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