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Reference type: Journal
Authors: Hu Y, Xia QF, Huang W, Hou XY, Tian MM
Article Title: Boronate-modified hollow molecularly imprinted polymers for selective enrichment of glycosides.
Publication date: 2018
Journal: Microchimica Acta
Volume: 185
Issue: (1)
Page numbers: ArticleNo46.
DOI: 10.1007/s00604-017-2608-2

Abstract: D-Glucose was used as a dummy template in a strategy to fabricate boronate-based hollow molecularly imprinted polymers (h-MIPs) for the recognition of glycosides. 3-Aminophenylboronic acid (APBA) was selected as the functional monomer to impart glycoside binding capability. A polystyrene core was synthesized via an emulsifier-free emulsion polymerization. It was then be corroded to form a hollow structure where the binding sites on the inner surface can be fully utilized. Adsorption studies indicate that the resulting h-MIPs can specifically recognize glycosides. The h-MIPs were applied as a sorbent for solid phase extraction of the glycosides (daidzin, glycitin, rutin, and genistin) in soy products. Following desorption with 1% TFA in acetonitrile-water (3:7, v/v), the glycosides were quantified by HPLC with UV detection. The detection limits for the glycosides range from 3.5 to 10.8 ng mL-1
Template and target information: glucose, D-glucose, glycosides, daidzin, glycitin, rutin, genistin
Author keywords: D-glucose Dummy template H-MIPs APBA PS Sorbent Soy products

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