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Reference type: Journal
Authors: Bhawani SA, Sen TS, Ibrahim MNM
Article Title: Synthesis of molecular imprinting polymers for extraction of gallic acid from urine.
Publication date: 2018
Journal: Chemistry Central Journal
Volume: 12
Issue: (1)
Page numbers: ArticleNo19.
DOI: 10.1186/s13065-018-0392-7

Abstract: The molecularly imprinted polymers for gallic acid were synthesized by precipitation polymerization. During the process of synthesis a non-covalent approach was used for the interaction of template and monomer. In the polymerization process, gallic acid was used as a template, acrylic acid as a functional monomer, ethylene glycol dimethacrylate as a cross-linker and 2,2'-azobisisobutyronitrile as an initiator and acetonitrile as a solvent. The synthesized imprinted and non-imprinted polymer particles were characterized by using Fourier-transform infrared spectroscopy and scanning electron microscopy. The rebinding efficiency of synthesized polymer particles was evaluated by batch binding assay. The highly selective imprinted polymer for gallic acid was MIPI1 with a composition (molar ratio) of 1:4:20, template: monomer: cross-linker, respectively. The MIPI1 showed highest binding efficiency (79.50%) as compared to other imprinted and non-imprinted polymers. The highly selective imprinted polymers have successfully extracted about 80% of gallic acid from spiked urine sample
Template and target information: gallic acid, GA
Author keywords: Gallic acid (GA), human urine, Molecular imprinting polymers (MIPs), acrylic acid, ethylene glycol dimethacrylate


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