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Reference type: Journal
Authors: He XP, Lian ZR, Wang JT
Article Title: Selective separation and purification of +-estradiol from marine sediment using an optimized core-shell molecularly imprinted polymer.
Publication date: 2018
Journal: Journal of Separation Science
Volume: 41
Issue: (20)
Page numbers: 3848-3854.
DOI: 10.1002/jssc.201800722

Abstract: The core-shell molecularly imprinted polymers were optimized to provide reliable connections that allow molecularly imprinted polymers to be fixed on SiO2 surface for the efficient separation and purification of β-estradiol from marine sediment for the first time. To achieve the goal, different preparation methods were used and finally the polymer using 3-methacryloxypropyltrimethoxysilane as coupling agent exhibited the best result, which further confirmed that 3-methacryloxypropyltrimethoxysilane played an indispensable role on improving the inter-particle connections. An offline molecularly imprinted solid-phase extraction with high-performance liquid chromatography method was successfully applied to the isolation and enrichment of β-estradiol from marine sediment samples with high adsorption capacity, excellent clean-up efficiency, and great enrichment effect as well as high recovery (>90%) and accuracy (RSD < 8.5%, n = 3). It proved the successful grafting of molecularly imprinted polymers on SiO2 surface and the applicability of the offline molecularly imprinted solid-phase extraction method in the selective extraction and enrichment of β-estradiol from marine sediment
Template and target information: β-estradiol, E2
Author keywords: Core-shell molecularly imprinted polymers, estradiol, marine sediment, Specific recognition


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