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Reference type: Journal
Authors: Wu XQ, Shen SG, Yan HY, Yuan YN, Chen X
Article Title: Efficient enrichment and analysis of atrazine and its degradation products in Chinese Yam using accelerated solvent extraction and pipette tip solid-phase extraction followed by UPLC-DAD.
Publication date: 2021
Journal: Food Chemistry
Volume: 337
Article Number: 127752.
DOI: 10.1016/j.foodchem.2020.127752
Alternative URL: https://www.sciencedirect.com/science/article/pii/S0308814620316149

Abstract: The Chinese Yam (Dioscorea opposita) is cultivated widely in China. However, there are potential safety risks associated with herbicide residues in Chinese Yam because of its characteristics and unregulated use of pesticides. We developed an efficient sample preparation technique for simultaneous analysis of atrazine and its degradation products in Chinese Yam using accelerated solvent extraction and pipette tip solid-phase extraction followed by UPLC-DAD analysis. Molecularly imprinted polymer (MIP) were used as the adsorbent material. Method performance was evaluated and our results showed the limit of quantification was 1-3 μg/ kg, with recoveries in the range 79.2-103.8%. When compared with other methods, this method provided superior performance in terms of sensitivity, accuracy, and precision. This method is, therefore, expected to be useful in supervised residue analysis
Template and target information: atrazine
Author keywords: Chinese Yam, atrazine, Accelerated solvent extraction, pipette tip solid-phase extraction, molecularly imprinted polymer


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