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Reference type: Journal
Authors: Zhang J, He LC, Fu Q
Article Title: Preparation of strychnine molecularly imprinted monolithic column.
Publication date: 2005
Journal: Chinese Journal of Analytical Chemistry
Volume: 33
Issue: (1)
Page numbers: 113-116.
Alternative URL: http://journal.9med.net/upload/pdf/132/1421/85969_1706.pdf

Abstract: Using strychnine as the template, methacrylic acid (MAA) as the functional monomer, ethylene glycol dimethacrylate ( EDMA) as the cross-linker, a strychnine imprinted monolithic column was prepared for the separation of the strychnine and brucine by in-situ, molecular imprinted technique. Then, the synthesis condition was optimized. The result showed the best ratio of template, functional monomer and cross-link was 1:4:16, and the toluene content in porogen was 18%. The effects of mobile phase composition, flow rate and column temperature on retention and separation factor were investigated. The maximum separation factor between strychnine and brucine was 3.5
Template and target information: strychnine
Author keywords: molecularly imprinted, strychnine, brucine, in-situ polymerization


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