Paper 3507

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Reference type: Journal
Authors: Schirmer C, Meisel H
Article Title: Synthesis of a molecularly imprinted polymer for the selective solid-phase extraction of chloramphenicol from honey.
Publication date: 2006
Journal: Journal of Chromatography A
Volume: 1132
Issue: (1-2)
Page numbers: 325-328.
DOI: 10.1016/j.chroma.2006.09.032
Alternative URL: http://www.sciencedirect.com/science/article/B6TG8-4M1DB2C-8/2/b5a293511c7bc3813c1f7908863e9502

Abstract: Solid-phase extraction (SPE) with a molecularly imprinted polymer (MIP) as sorbent has been investigated for the clean-up of the broad-spectrum bacteriostatic antibiotic chloramphenicol (CAP) in honey samples. The MIP was prepared by using methacrylic acid (MAA) as functional monomer, ethylene glycol dimethacrylate (EDMA) as cross-linker, chloroform as porogen and CAP as template molecule. The binding behaviour of the template CAP on the MIP was evaluated by high-performance liquid chromatography, and then the MIP was applied as a sorbent in SPE to selectively extract CAP from honey. It was shown that recoveries of nearly 100% of a CAP standard solution and up to 94% from spiked honey samples could be obtained after SPE
Template and target information: chloramphenicol, CAP
Author keywords: molecular imprinting, Solid-phase extraction, chloramphenicol, Honey samples

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