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Reference type: Journal
Authors: Zhou L, Ye GR, Yuan R, Chai YQ, Chen SM
Article Title: A capacitive sensor based on molecularly imprinted polymers and poly(p-aminobenzene sulfonic acid) film for detection of pazufloxacin mesilate.
Publication date: 2007
Journal: Science in China Series B: Chemistry
Volume: 50
Issue: (4)
Page numbers: 547-553.
DOI: 10.1007/s11426-007-0035-7
Alternative URL: http://chem.scichina.com:8081/sciBe/EN/abstract/abstract398769.shtml

Abstract: A novel capacitive sensor for pazufloxacin mesilate (pazufloxacin) determination was developed by electropolymerizing p-aminobenzene sulfonic (p-ABSA) and molecularly imprinted polymers (MPs), which was synthesized through thermal radical copolymerization of metharylic acid (MAA) and ethylene glycol dimethacrylate (EGDMA) in the presence of pazufloxacin template molecules, on the gold electrode surface. Furthermore, 1-dedecanethiol was used to insulate the modified electrode. Alternating current (ac) impedance experiments were carried out with a Model IM6e to obtain the capacitance responses. Under the optimum conditions, the sensor showed linear capacitance response to pazufloxacin in the range of 5 ng mL-1 to 5 μg mL-1 with a relative standard deviation (RSD) 5.3% (n=7) and a detection limit of 1.8 ng mL-1. The recoveries for different concentration levels of pazufloxacin samples varied from 94.0% to 102.0%. Electrochemical experiments indicated the capacitive sensor exhibited good sensitivity and selectivity and showed excellent parameters of regeneration and stability
Template and target information: pazufloxacin mesilate, pazufloxacin
Author keywords: capacitive sensor, Molecularly imprinted polymers, p-aminobenzene sulfonic acid, pazufloxacin mesilate


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