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Reference type: Journal
Authors: Zhuang Y, Luo HP, Duan DL, Chen LR, Xu XJ
Article Title: In situ synthesis of molecularly imprinted polymers on glass microspheres in a column.
Publication date: 2007
Journal: Analytical and Bioanalytical Chemistry
Volume: 389
Issue: (4)
Page numbers: 1177-1183.
DOI: 10.1007/s00216-007-1526-2

Abstract: A facile method to fabricate molecularly imprinted polymers (MIPs) on glass microspheres in a column was developed. The column was prepacked with glass microspheres, and then the prepolymerization mixture was injected into the interstitial volume of the column. The polymerization took place in situ and the column could be directly used for high-performance liquid chromatography after the template had been removed. The template consumption was reduced greatly because the prepolymerization mixture just filled the interstitial volume between the glass microspheres in the column. The MIPs obtained exhibited better kinetic properties, higher efficiency, and low back pressure of the column. Emodin imprinted polymers were prepared by this method and were used for solid-phase extraction
Template and target information: emodin
Author keywords: molecularly imprinted polymer, In-column, Glass microsphere, Emodin, Solid-phase extraction


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