MIPdatabase
Authors: Wang RY, Wang PL, She YX, Wang J, Wang XC, Zhong YG
Article Title: Study on the determination of trace chloramphenicol residue in milk by HPLC with matrix solid-phase dispersion using molecularly imprinted polymer as an adsorbent.
Publication date: 2009
Journal: Chinese Journal of Analysis Laboratory
Volume: 28
Issue: (8)
Page numbers: 26-28.
Alternative URL: http://en.cnki.com.cn/Article_en/CJFDTotal-FXSY200908008.htm
Abstract: The CAP was extracted by MSPD using molecularly imprinted polymer of CAP,the clean procedure was performed using HLB solid phase extraction cartridge and the quantitative analysis was carried out by HPLC.The clean effect of MSPD was examined.The results indicated that the limit of detection(LOD) and limit of quantity(LOQ) were 0.15 and 0.50 ng/mL respectively under optimum conditions.The developed method was applied to the determination of CAP in milk,the recoveries of different quantities of CAP are above 93.2%,and the relative standard deviations(RSD) is below 5.9%.This method possesses the merits of convenient operation,high sensitivity,good repeatability,and no need for abundant solvents,which is a feasible method for analysis of CAP in milk samples.
Template and target information: chloramphenicol, CAP
Author keywords: chloramphenicol, molecularly imprinted polymer, Matrix solid-phase dispersion, HPLC, milk
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