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Reference type: Journal
Authors: Wang H, Yan HY, Qiu MD, Qiao JD, Yang GL
Article Title: Determination of dicofol in aquatic products using molecularly imprinted solid-phase extraction coupled with GC-ECD detection.
Publication date: 2011
Journal: Talanta
Volume: 85
Issue: (4)
Page numbers: 2100-2105.
DOI: 10.1016/j.talanta.2011.07.061
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0039914011006369

Abstract: The novel molecularly imprinted microsphere (MIM) that could be applied as special sorbent was synthesized by aqueous suspension polymerization using 1,1-bis(4-chlorophenyl)-1,2,2,2-tetrachloroethane (α-chloro-DDT) as the dummy template. The obtained MIM exhibited good recognition and selectivity to dicofol and it was successfully applied as selective sorbent of solid-phase extraction for the determination of dicofol from aquatic products. At the optimum conditions of the molecularly imprinted solid-phase extraction (MISPE) coupled with GC-ECD, good linearity for dicofol was achieved in a range of 0.4-100 ng g-1 (r2 = 0.9995) and the recoveries at three spiked levels were ranged from 85.8% to 101.2% for aquatic products with the relative standard deviation (RSD) less than 5.6%. The presented MISPE-GC-ECD method exhibited the advantages of simplicity, selectivity and sensitivity, and could be potentially applied to the determination of dicofol in complicated aquatic products
Template and target information: 1,1-bis(4-chlorophenyl)-1,2,2,2-tetrachloroethane, α-chloro-DDT, dummy template, dicofol
Author keywords: molecularly imprinted microspheres, Dummy template polymerization, Solid-phase extraction, Dicofol, Aquatic products


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