MIPs logo MIPdatabase      Use this space
Custom Search
Reference type: Journal
Authors: Golsefidi MA, Es'haghi Z, Sarafraz-Yazdi A
Article Title: Design, synthesis and evaluation of a molecularly imprinted polymer for hollow fiber - solid phase microextraction of chlorogenic acid in medicinal plants.
Publication date: 2012
Journal: Journal of Chromatography A
Volume: 1229
Issue: (1)
Page numbers: 24-29.
DOI: 10.1016/j.chroma.2012.01.019
Alternative URL: http://www.sciencedirect.com/science/article/pii/S0021967312001021

Abstract: In this study, a simple preparation approach was developed for modified bisphenol A (BPA) molecularly imprinted polymer sorbent used in the hollow fiber solid phase microextraction (MIP-HF-SPME) of chlorogenic acid (CGA). The pre-polymer solution containing the template was introduced into the polypropylene hollow fiber segment for in situ polymerization. MIP-HF-SPME conditions based on the modified MIP-sorbent were optimized. Finally, the tool was used for selective extraction of chlorogenic acid in Echinacea purpurea, a medicinal plant. Main parameters affecting synthesis of organic-inorganic hybrid MIP and microextraction procedure were investigated and optimized. The measurements were done under the optimal conditions. The limit of detection has been gained 0.08 ng/mL. The linear range and relative standard deviation (RSD %) are 0.2 - 1000 ng/mL and 0.38 (n = 3) respectively. The average relative recoveries of spiked analyte in the four concentration levels were between 84.8 and 97.2%
Template and target information: bisphenol A, BPA, chlorogenic acid, CGA
Author keywords: chlorogenic acid, Hollow fiber solid phase microextraction, Molecularly imprinted polymers


  Mister Benzene shirt  Chemistry peptide mug    Mug featuring the template Bisphenol A

Molecules Special Issue call      Appeal for information






 

Join the Society for Molecular Imprinting
Logo of the Society for Molecular Imprinting

New items RSS feed
new items RSS feed  View latest updates

Sign-up for e-mail updates:
Choose between receiving an occasional newsletter or more frequent e-mail alerts.
Click here to go to the sign-up page.


Is your name elemental or peptidic? Enter your name and find out by clicking either of the buttons below!
Other products you may like:
view listings for MIP books on eBay:



Mickey Mouse 90th Anniversary banner