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Reference type: Journal
Authors: Bianchi F, Giannetto M, Mori G, D'Agostino G, Careri M, Mangia A
Article Title: Solid-phase microextraction of 2,4,6-trinitrotoluene using a molecularly imprinted-based fiber.
Publication date: 2012
Journal: Analytical and Bioanalytical Chemistry
Volume: 403
Issue: (8)
Page numbers: 2411-2418.
DOI: 10.1007/s00216-012-5875-0

Abstract: A molecularly imprinted polymer with trinitrotoluene as the template molecule was synthesized and used as the novel coating for solid-phase microextraction of the nitroaromatic explosive 2,4,6-trinitrotoluene for its selective determination. The fiber was characterized in terms of coating thickness, morphology, intra- and inter-batch repeatability and extraction efficiency. An average thickness of 50 4 μm with a uniform distribution of the coating was obtained. Good performances of the developed procedure in term of both intra-batch and inter-batch repeatability with relative standard deviations < 8% were obtained. Finally, detection and quantitation limits in the low nanogram per kilogram levels were achieved proving the superior extraction capability of the developed coating, obtaining gas chromatography-mass spectrometry responses about two times higher than those achieved using commercial devices.
Template and target information: TNT, 2,4,6-trinitrotoluene
Author keywords: solid-phase microextraction, molecularly imprinted polymer, 2,4,6-Trinitrotoluene, coating, Explosives


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