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Reference type: Journal
Authors: Matejicek D, GrycovŠ A, Vlcek J
Article Title: The use of molecularly imprinted polymers for the multicomponent determination of endocrine-disrupting compounds in water and sediment.
Publication date: 2013
Journal: Journal of Separation Science
Volume: 36
Issue: (6)
Page numbers: 1097-1103.
DOI: 10.1002/jssc.201200992

Abstract: The method employing molecularly imprinted polymers for the extraction and clean up of endocrine-disrupting compounds (estrogens, bisphenol A, and alkylphenols) from water and sediment is described. The identical extraction/clean-up and LC-MS/MS condition were used for the analysis of both types of samples. The method showed high recoveries ranging from 90 to 99% with excellent precision (intrabatch: 3.6 - 9.3%; interbatch: 5.6 - 11.4% for water; intrabatch: 4.3 - 8.5%; interbatch: 6.1 - 9.6% for sediment). The LOD was in the range of 0.7 - 1.9 ng/L and 0.3 - 0.6 ng/g for water and sediment, respectively. Overall extraction on molecularly imprinted polymers substantially enhanced sample clean-up. The difference in efficiency of clean-up was particularly pronounced when a large sample volume/weight was extracted and analyzed. Finally, the method was successfully applied for the analysis of 20 water and sediment samples
Template and target information: endocrine-disrupting compounds, estrogens, bisphenol A, alkylphenols
Author keywords: endocrine-disrupting compounds, Molecularly imprinted polymers, Sediment, water


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