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Reference type: Journal
Authors: Lee TP, Saad B, Salleh B, Mat I
Article Title: Micro-solid phase extraction of ochratoxin A, and its determination in urine using capillary electrophoresis.
Publication date: 2013
Journal: Microchimica Acta
Volume: 180
Issue: (11-12)
Page numbers: 1149-1156.
DOI: 10.1007/s00604-013-1042-3

Abstract: We describe a simple, environmentally friendly and selective technique for the determination of ochratoxin A (OTA) in urine. It involves (a) the use of a molecularly imprinted polymer as a sorbent in micro-solid-phase extraction in which the sorbent is contained in a propylene membrane envelope, and (b) separation and detection by capillary electrophoresis (CE). Under optimized conditions, response is linear in the range between 50 and 300 ng mL-1 (with a correlation coefficient of 0.9989), relative standard deviations range from 4 to 8 %, the detection limit for OTA in urine is 11.2 ng mL-1 (with a quantification limits of 32.5 ng mL-1) which is lower than those of previously reported methods for solid-phase extraction combined with CE. The recoveries of OTA from urine spiked at levels of 50, 150 and 300 ng mL-1 ranged from 93 to 97 %
Template and target information: ochratoxin A, OTA
Author keywords: ochratoxin A, molecularly imprinted polymer, Micro-solid phase extraction, capillary electrophoresis, urine


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